English
Русский 15-20 p.
The aim of the work was the development of a sorption-atomic-absorption method for determining mercury after its separation from wine samples in the form of a complex with unithiol on modified polyhexamethylene guanidine silica. The sorption-atomic absorption determination of mercury in wines was performed using the cold-steam method. The developed method is characterized by a low detection limit and a sufficiently high accuracy and satisfactory reproducibility.
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2. Dressler V.L. Total mercury, inorganic mercury and methyl mercury determination in red wine // Food Anal. Methods. 2012. №5. R. 505 – 511.
3. Karadjova I., Arpadjan, S. Cvetkoviґ c J., Stafilov T. Sensitive method for trace determination of mercury in wines using electrothermal atomic absorption spectrometry // Microchim. Acta. 2004. №147. R. 39 – 43.
4. Leopold K. Methods for the determination and speciation of mercury in natural waters – a revie // Anal. Chim. Acta. 2010. №663. R. 127 – 138.
5. Martinis E.M. Cold vapor ionic liquid-assisted headspace singledrop microextraction: a novel preconcentration technique for mercury species determination in complex matrix samples // J. Anal. At. Spectrom. 2010. №25. R. 1432 – 1439.
6. Wulff G. Molecular imprinting in cross-linked materials with the aid of molecular templates – a way towards artificial antibodies // Angew. Chem. Int. Ed. Engl. 1995. №34. R. 1812 – 1832.11.